PHARMACEUTICAL INORGANIC CHEMISTRY LAB SYLLABUS 2009-10

PHARMACEUTICAL INORGANIC CHEMISTRY LAB
SYLLABUS 2009-10

B. Pharmacy I Year
P C
3 4

JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY
ANANTAPUR.

PHARMACEUTICAL INORGANIC CHEMISTRY LAB
List of experiments:
A) Limit tests for the following as per the procedure given in Indian Pharmacopoeia (1996 – including the latest addenda)





1) Chlorides
2) Sulphates
3) Heavy metals
4) Iron
5) Arsenic
6) Modifications in limit test for chlorides and sulphates in potassium
permanaganate, sodium bicarbonates, sodium benzoates and sodium salicylates.


B)
7)Balances and Weighing; Calibration of weights, Pipette and Burette.
8)Preparation and standardization of Hydrochloric acid solution (0.1N).
9)Preparation and standardization of Potassium permanganate solution (0.1N &
0.1M).
10)Preparation of a primary standard solution of 0.1N Potassium hydrogen-
phthalate.

11)Preparation and standardization of 0.1N EDTA solution.
12)Preparation and purification of Boric acid.
13)Preparation and purification of Sodium citrate.
14)Preparation and purification of Potash alum.
15)Preparation and purification of Magnesium stearate.
16)Assay of sodium bicarbonate and assay of Boric acid (Neutralization).
17)Assay of Calcium gluconate (or) any calcium compounds (Complexometry).
18)Assay of Copper sulphate (Redox titration).
19)Assay of Sodium acetate (Non-aqueous titration).
20)Assay of Ferrous sulphate (Oxidation-reduction / Redox titration).
21)Swelling power in bentonite
22)Test for purity (Ammonium salts in potash alum, presence of iodates in KI)

REFERENCES

1. Indian Pharmacopoeia - 1996.
2. Vogel’s Qualitative Analysis


LIST OFMINIMUM EQUIPMENT REQUIRED

1. Analytical balances
2. Physical balances
3. Suction pumps
4. Oven
5. Hot plates
6. Water baths
7. Distillation unit
8. Limit test apparatus for arsenic
9. Adequate glasswares